N-Methyl-4-(4-pivalamidophenylsulfanyl)picolinamide hemihydrate

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N-Methyl-4-(4-pivalamido­phenyl­sulfan­yl)picolinamide hemihydrate

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In the title compound, C(16)H(17)N(3)O(2)·0.5H(2)O, the two hydrazide mol-ecules are approximately planar: the dihedral angles between the two substituted benzene rings are 7.7 (2) and 4.2 (2)°. Both hydrazone mol-ecules exist in a trans geometry with respect to their methyl-idene units. In the crystal, the water mol-ecule lies between the two organic mol-ecules and makes bifurcated O-H⋯(N,O) h...

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The title compound, C(18)H(12)N(2)O(2)·0.5H(2)O, was prepared by the reaction of 1,4-phenyl-enediamine with 1,8-naphthalic anhydride in refluxing dimethyl-formamide. The structure is stabilized by N-H⋯O and O-H⋯O hydrogen bonds. There are π-π stacking inter-actions [centroid-centroid distances of 3.718 (2), 3.510 (2) and 3.546 (2) Å] and C-H⋯π inter-actions between the mol-ecules. The water mol...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2011

ISSN: 1600-5368

DOI: 10.1107/s1600536811012268